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X-Ray Structure Determination: A Practical Guide, 2nd Edition, by George H. Stout, Lyle H. Jensen
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Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
- Sales Rank: #1123703 in Books
- Published on: 1989-04-24
- Original language: English
- Number of items: 1
- Dimensions: 9.51" h x 1.59" w x 6.34" l, 1.68 pounds
- Binding: Hardcover
- 480 pages
From the Publisher
Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
Most helpful customer reviews
7 of 8 people found the following review helpful.
introduction to the basics, at least in theory
By Edmund Paley
This book is an excellent excellent introction to the basic physics and math of x-ray crystallography. This was used as the text in an undergrad class I took on protein crystallography and it was perfect for that purpose. The main drawback of this book is that it is really concentrated on small molecule structure determination, and doesn't address the problems or specific techniques used for large protein structures. So probably the best way to use this book would be in conjuction with a more protein-specific book. But for the raw fundamentals of symmetry and diffraction, I don't think you can beat stout & jensen.
2 of 2 people found the following review helpful.
Probably the best introduction to X-ray structure determination of small-molecule crystals written so far
By Pichierri Fabio
The book of Stout and Jensen (2-nd edition, 1989) is, in my opinion, the best introduction to X-ray structure determination (of small molecule crystals) written so far. Why? Because it is clearly written while keeping in mind many practical aspects without, however, neglecting the theoretical foundations. The book is organized in three parts and 19 chapters along with five appendices. The most modern (post 1980s) instrumentation (image plate, CCD, etc.) is not covered but this is not a problem, I think, for the necessary information can easily be obtained either from manuals or the internet. Those that are interested in protein crystallography should consult specialized books such as Drenth's Principles of Protein X-Ray Crystallography or Rupp's Biomolecular Crystallography: Principles, Practice, and Application to Structural Biology. A slightly more advanced treatment of X-ray analysis can be found in Dunitz's book X-Ray Analysis and the Structure of Organic Molecules (the corrected reprint of the 1979 edition was published in 1996).
0 of 0 people found the following review helpful.
Excellent Reference!!!
By J Guerra
Excellent Reference!!!
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